Kinetics Experiments on the Bruker 500

Following is a 31P kinetics spectrum run on the 500, collected by Zak Page. Over the course of the reaction, the decrease of the reactant peaks at 28 ppm, the increase of the product peaks at 1 ppm, and the first increase, then decrease of the intermediate signal at 27 ppm can be clearly seen. The time scale of the F1 dimension is erroneous (a software glitch).

kinetics-31P-ZakPage